X射线衍射分析实例.doc

No.
Pos. [°2Th.]
FWHM [°2Th.]
d-spacing [?]
Height [cts]
Rel. Int. [%]
1
31.8347
0.576

360.77

2
34.3965
0.576

234.65

3
36.2286
0.576

568.57

4
47.5674
0.768

87.49

5
56.4988
0.384

209.02

6
62.7255
0.96

108.74

7
67.9427
0.48

102.66

8
76792
1.152

17.97

注：Dhkl=0.89λ/(Bcosθ)，其中，λ=1.54050Å，B为宽化系数，B2 = Bm2 - Bs2，Bm为待测样品衍射峰的半高宽（弧度），Bs为标准样品衍射峰的半高宽（弧度）。

Reference code: 00-048-1066

PDF index name: Zinc Hydroxide

Chemical formula: Zn (OH)2

Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 1 0 2.81150 31.803 59.0
2 0 0 6 2.60090 34.455 63.0
3 1 1 3 2.47370 36.287 100.0
4 3 0 0 1.62590 56.558 25.0
5 1 1 9 1.47740 62.851 26.0

Reference code: 03-065-0369

PDF index name: Europium

Chemical formula: Eu

Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 0 0 2.83450 31.538 25.4
2 0 0 2 2.54150 35.286 24.2
3 1 0 1 2.47560 36.258 100.0
4 1 0 2 1.89225 48.043 12.9
5 1 1 0 1.63650 56.159 14.7
6 1 0 3 1.45432 63.965 13.2
7 2 0 0 1.41725 65.847 2.0
8 1 1 2 1.37593 68.089 14.0
9 2 0 1 1.36518 68.700 10.2
10 0 0 4 1.27075 74.627 1.6
11 2 0 2 1.23780 76.971 2.2
12 1 0 4 1.15955 83.259 1.6

Reference code: 01-089-7102

ICSD name: Zinc Oxide

Chemical formula:ZnO

Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 0 0 2.81415 31.772 55.8
2 0 0 2 2.60345 34.420 39.3
3 1 0 1 2.47570 36.256 100.0
4 1 0 2 1.91107 47.541 19.7
5 1 1 0 1.62475 56.602 28.5
6 1 0 3 1.47726 62.858 25.3
7 2 0 0 1.40707 66.384 3.6
8 1 1 2 1.37836 67.953 19.0
9 2 0 1 1.35835 69.094 9.7
10 0 0 4 1.30173 72.563 1.5
11 2 0 2 1.23785 76.967 2.8
12 1 0 4 1.18145 81.384 1.4
13 2 0 3 1.09301 89.619 5.8

Reference code: 01-089-2803

ICSD name: Cobalt Oxide

Chemical formula: CoO

Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 0 0 2.77994 32.173 62.3
2 0 0 2 2.62000 34.196 44.5
3 1 0 1 2.45575 36.561 100.0
4 1 0 2 1.90666 47.658 21.0
5 1 1 0 1.60500 57.363 29.8
6 1 0 3 1.47897 62.777 27.6
7 2 0 0 1.38997 67.309 3.8
8 1 1 2 1.36861 68.504 18.9
9 2 0 1 1.34351 69.968 8.9
10 0 0 4 1.31000 72.033 1.4
11 2 0 2 1.22787 77.709 2.8
12 1 0 4 1.18502 81.088 1.3

Reference code: 00-040-1275

PDF index name: Zirconium Nitride

Chemical formula: ZrN0.28

Peak list
No. h k l d [A] 2Theta[deg] I [%]
1 1 0 0 2.79000 32.054 20.0
2 0 0 2 2.58800 34.632 24.0
3 1 0 1 2.45600 36.557 100.0
4 1 0 2 1.89700 47.915 18.0
5 1 1 0 1.61100 57.129 19.0
6 1 0 3 1.46700 63.348 20.0
7 2 0 0 1.39500 67.034 2.0
8 1 1 2 1.36800 68.539 19.0
9 2 0 1 1.34700 69.761 15.0
10 0 0 4 1.29400 73.066 3.0
11 2 0 2 1.22800 77.699 4.0
12 1 0 4 1.17400 82.011 3.0